The Synthesis, Characterization Gd(Iii) Complex with Heptilmethyl- Ditiocarbamate and 2,9-Dimethyl Phenanthroline as Anti-Tuberculosis

Muhammad Arham Yunus (1), Raya Indah (2), Nurfiansyah Nurfiansyah (3), Septiani Mimin (4)
(1) Universitas Hasanuddin post graduate, Indonesia,
(2) Department of Chemistry, Faculty of Mathematics, and Natural Science, Hasanuddin University, Makassar 90245, South Sulawesi, Indonesia, Indonesia,
(3) Department of Chemical Engineering, Ujung Pandang State Polytechnic, Makassar 90254, South Sulawesi, Indonesia, Indonesia,
(4) Department of Chemical Engineering, Ujung Pandang State Polytechnic, Makassar 90254, South Sulawesi,Indonesia, Indonesia
https://doi.org/10.20956/ica.v16i1.26900

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Issue
Volume 16, No 1: June 2023
Submitted
May 28, 2023
Accepted
August 15, 2023
Published
August 28, 2023
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Abstract

Mycobacterium tuberculosis is a bacterium that causes tuberculosis infection disease. The aim of this study was to produce complex compounds that have the ability to damage the cell wall of Mycobacterium tuberculosis. Gd(III)Heptylmethyldithiocarbamate 2,9-dimethyl phenanthroline complex was synthesised and characterised by reacting N-heptylmethylamine, carbondisulphide, 2,9-dimethyl phenanthroline and lanthanide group metal ion (Gadolinium) using in situ method. Characterisation was carried out using electrothermal melting point, conductometer, UV-Vis spectrophotometer, and FT-IR spectrophotometer. The resulting Gd(III)Heptylmethyldithiocarbamate 2,9-dimethyl phenanthroline complex was white in colour as much as 7.01%, conductivity 20 Ω-1 and melting point 208-210o C. Testing of complex compounds gave effective results as antibacterial Mycobacterium tuberculosis.

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Authors

Muhammad Arham Yunus
Universitas Hasanuddin post graduate
arhamyunus21@gmail.com (Primary Contact)
Raya Indah
Department of Chemistry, Faculty of Mathematics, and Natural Science, Hasanuddin University, Makassar 90245, South Sulawesi, Indonesia
Nurfiansyah Nurfiansyah
Department of Chemical Engineering, Ujung Pandang State Polytechnic, Makassar 90254, South Sulawesi, Indonesia
Septiani Mimin
Department of Chemical Engineering, Ujung Pandang State Polytechnic, Makassar 90254, South Sulawesi,Indonesia
Yunus, M. A., Indah, R., Nurfiansyah, N., & Mimin , S. (2023). The Synthesis, Characterization Gd(Iii) Complex with Heptilmethyl- Ditiocarbamate and 2,9-Dimethyl Phenanthroline as Anti-Tuberculosis. Jurnal Akta Kimia Indonesia (Indonesia Chimica Acta), 16(1), 9–12. https://doi.org/10.20956/ica.v16i1.26900
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